Yellow Solution Sample Clauses

Yellow Solution. Dissolve 46g of ferric chloride R in about 900ml of a mixture of 25ml of hydrochloric acid R and 975ml of water (0.3N hydrochloric acid) and dilute to 1000ml with this mixture. Place 10ml of solution, 15ml of water, 5ml hydrochloric acid R and 4g of potassium iodide into a 250ml stoppered conical flask. Allow to stand in the dark for 15 minutes and add 100ml of water. Titrate the liberated iodine with standardised 0.1N sodium thiosulphate. Towards the end of the titration when the solution is a light yellow colour (about 16ml) add 0.5ml of starch indicator, continue the titration until the blue colour has gone. Calculate the concentration of the solution using the following equation: FeCl(3)6H(2)0(mg/ml) = mls of Na(2)S(2)0(3) x N of Na(2)S(2)0(3) x 27.03mg Adjust the concentration to within 10% of 45mg/ml by diluting with 0.3N hydrochloric acid using the calculation below. [LOGO] Authorized: [**] (MICRONISED IR) Page 8 of 19 METHOD OF ANALYSIS No: [**]Version 3 ml of 0.3N HCl per 100ml of yellow solution = 100 - 4500 -------------------- FeCl(3)6H(2)0 mg/ml
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