Effect of of annealing temperature Sample Clauses

Effect of of annealing temperature. Intensity (a.u.) For this study, we have selected the sample prepared with Bi/Mn ratio of 0.3, CaO amount of 30% and Ca/O ratio of 1.18 because it showed higher Ms and Hc values. The first annealing step was performed at different temperatures, i.e. 800°C /5 m, 900°C /5 m and 1200°C /3 m, then the second annealing step was done at 300°C for 15 h. Figure 8 shows the XRD patterns of the MnBi nanoparticles annealed at different temperatures. With increase of annealing temperature, the volume fraction of the MnBi phase increases and this increase is also reflected in the magnetization curves (Fig. 9) which clearly show higher Ms values. The effect of annealing temperature on particle size is shown in Fig. 10. As seen from SEM images, the average particle size increases from 200 nm to 2 µm as the annealing temperature increases from 800°C to 1200°C. Bi MnBi 1200C/3 min 900C/5 min 800C/5 min 25 30 35 40 45 50 55 2θ(deg.) Fig. 8. XRD patterns of MnBi particles annealed at different temperatures.
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