IF NITROGEN AND/OR SULFUR PRESENT Sample Clauses

IF NITROGEN AND/OR SULFUR PRESENT. If either nitrogen or sulfur is present, the cyanide and sulfide ions must first be removed. Acidify ~ 0.5 mL of the filtrate with dilute nitric acid and concentrate to half of its original volume to expel any hydrogen cyanide or hydrogen sulfide that might be present in the mixture (CAUTION: carry out the reactions in a fume cupboard). Dilute the mixture with an equal volume of distilled water. Add 1-2 drops 5% of aqueous silver nitrate solution to 2-3 mL of the fusion solution. An immediate heavy precipitation indicates the presence of chlorine, bromine, or iodine.
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