LLZO Characterization Sample Clauses

LLZO Characterization. Besides multistructural characterization (1.1), LLZO-powders will also be subjected to other physical-chemical characterizations at FhG IKTS, namely of phase purity by X-ray diffraction (XRD) and ionic conductivity (Electrochemical Impedance Spectroscopy (EIS).
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LLZO Characterization. Besides multistructural characterization (1.1), LLZO-powders will also be subjected to other physical-chemical characterizations at FhG IKTS, namely of phase purity by X-ray diffraction (XRD) and ionic conductivity (Electrochemical Impedance Spectroscopy (EIS). X-ray diffraction (XRD) The Al-doped LLZO powder is synthesized by solid state reaction. The starting materials La2O3, ZrO2, Li2CO3 and Al2O3 are mixed in water-free isopropanol, and calcined multiple times with subsequent milling. The LLZO powder is analyzed regarding it`s phase purity with XRD. The particle distribution is measured without dispersing agent in isopropanol. Electrochemical Impedance Spectroscopy (EIS) (Ionic conductivity) To determine the ionic conductivity pellets of the powder are pressed and sintered. The pellets with a density of > 90 % theoretical density are analyzed by impedance spectroscopy with blocking electrodes in the frequency range of 100 mHz to 1 MHz. The measurement is conducted in EL-ECC® cells with a Biologic potentiostat VMP3.

Related to LLZO Characterization

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