PbI2 dispersion Sample Clauses

PbI2 dispersion. In order to achieve a uniform PbI2 layer, the first task was to make a stable dispersion from the PbI2 powder. Typically, there are three approaches that can be followed when making a dispersion: 1) Charging the particles, 2) Separation of particles by a ligand, or 3) Increase the viscosity of the solution supporting the particles. At first, the approach of utilizing citric acid (and later also other materials) as a ligand separating the PbI2-particles from agglomerating was followed. The PbI2 pellets were ground to a fine powder with a ball mill and then dispersed in citric acid (CA) solution in ethanol by ultrasonication. Citric acid was chosen as the ligand that interacts with the PbI2 particles and prevents aggregation by keeping the particles separated from each other. Several PbI2 and citric acid concentrations were tested to improve stability of the ink (and the quality of the printed PbI2 layers) and these are listed in Table 1. Table 1. The tested lead iodide and citric acid concentrations.
Sample 1
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