Effect of amount of excess dispersant CaO Sample Clauses

Effect of amount of excess dispersant CaO. Intensity (a.u.) The amount of excess CaO was varied from 15-45% keeping constant a Ca/O ratio of 1.18 (this ratio was also optimized) and Bi/Mn ratio of 0.3. Annealing was done at 800°C /10 min followed by a long term annealing of powders at 300°C for 15 h. Figure 1 shows the XRD patterns of the washed MnBi nanoparticles prepared with different excess CaO. The powders consist of MnBi LTP and Bi phases. With increase of excess CaO, a lower volume Bi MnBi CaO=45% CaO=40% CaO=35% CaO=30% CaO=20% CaO=15% 25 30 35 40 45 50 55 2θ (deg.) Fig. 1. XRD patterns of the washed MnBi nanoparticles prepared with different excess CaO
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Related to Effect of amount of excess dispersant CaO

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