Calibration and hydrogen retention test of the chamber Sample Clauses

Calibration and hydrogen retention test of the chamber. The calibration and hydrogen retention test in the chamber provides a check on the calculated volume (paragraph 2.1) and also measures any leak rate. The enclosure leak rate must be determined at the enclosure's introduction to service, after any operations in the enclosure which may affect the integrity of the enclosure, and at least monthly thereafter. If six consecutive monthly retention checks are successfully completed without corrective action, the enclosure leak rate may be determined quarterly thereafter as long as no corrective action is required. 2.3.1. The enclosure must be purged until a stable hydrogen concentration is reached. The mixing fan is turned on, if not already switched on. The hydrogen analyser is zeroed, calibrated if required, and spanned. 2.3.2. The enclosure must be latched to the nominal volume position. 2.3.3. The ambient temperature control system is then turned on (if not already on) and adjusted for an initial temperature of 293 K. 2.3.4. When the enclosure temperature stabilizes at 293 K ± 2 K, the enclosure is sealed and the background concentration, temperature and barometric pressure measured. These are the initial readings CH2i, Ti and Pi used in the enclosure calibration. 2.3.5. The enclosure must be unlatched from the nominal volume. 2.3.6. A quantity of approximately 100 g of hydrogen is injected into the enclosure. This mass of hydrogen must be measured to an accuracy of ± 2 per cent of the measured value. 2.3.7. The contents of the chamber must be allowed to mix for five minutes and then the hydrogen concentration, temperature and barometric pressure are measured. These are the final readings CH2f, Tf and Pf for the calibration of the enclosure as well as the initial readings CH2i, Ti and Pi for the retention check. 2.3.8. On the basis of the readings taken in paragraphs 2.3.4 and 2.3.7 and the formula in paragraph 2.4, the mass of hydrogen in the enclosure is calculated. This must be within ± 2 per cent of the mass of hydrogen measured in paragraph 2.3.6. 2.3.9. The contents of the chamber must be allowed to mix for a minimum of
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