Equipment Rinsate Water Samples Sample Clauses

Equipment Rinsate Water Samples. Sample Preparation All equipment rinsate water samples (see Section B5.1.5) should be prepared for asbestos analysis in basic accordance with the techniques in EPA Method 100.2, as modified by Xxxxx Laboratory Modification LB-000020A. In brief, all water samples will be prepared using an ozone/ultraviolet treatment that oxidizes organic matter that is present in the water or on the walls of the bottle, destroying the material that causes clumping and binding of asbestos structures. Following treatment, an aliquot of water (generally about 50 milliliters) will be filtered through a 25-millimeter diameter polycarbonate filter with a pore size of 0.1 µm with a mixed cellulose ester filter (0.45 µm pore size) used as a support filter. Analysis Method and Counting Rules Approximately one quarter of the filter will be used to prepare a minimum of three grids using the grid preparation techniques described in Section 9.3 of ISO 10312:1995(E). Grids will be examined by TEM in basic accordance with the recording procedures described in ISO 10312:1995(E), as modified by the most recent versions of Xxxxx Laboratory Modifications LB-000016, LB-000029, LB-000066D, LB-000067, and LB-000085. All structures with fibrous morphology, an x-ray diffraction pattern consistent with amphibole asbestos, a energy dispersive spectrum consistent with LA, length ≥ 0.5 µm, and an aspect ratio (length:width) ≥ 3:1 will be counted and recorded. These counting rules will enable the calculation of water concentrations based on both total LA and LA structures longer than 10 µm. If observed, chrysotile structures will be recorded, but chrysotile structure counting may stop after 25 structures have been recorded. Stopping Rules The TEM stopping rules for equipment rinsate water samples from this investigation are specified below and were selected to be consistent with the analytical requirements specified in other water sampling efforts conducted at the Site. The stopping rules are as follows:
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