Analytical Methods and Requirements. This section discusses the analytical methods and requirements for tissue sampling program. Detailed information is included on the analysis of LA in the tissue samples, as well as sample preparation, and data reporting requirements. An analytical requirements summary sheet (TISSOU4-0812), which details the specific preparation and analytical requirements associated with this sampling program, is provided in Appendix D. The analytical requirements summary sheet will be reviewed and approved by all participating laboratories in this sampling program prior to any sample handling. A copy of this analytical requirements summary sheet will be submitted with each COC record.
Analytical Methods and Requirements. Information regarding the extraction, digestion, and analytical methodologies can be found in Pace Analytical’s Quality Assurance Manual (QAM), included electronically in Appendix D. Methods for metals can be found on page 13 of Appendix V of the QAM and semi-volatiles on page 21 of Appendix VII. Laboratory data is typically received within five business days of the laboratory’s receipt of the samples. However, for the purposes of this project, the air samples will rushed for analysis with an anticipated turnaround time of one day.
Analytical Methods and Requirements. This section discusses the analytical methods and requirements for samples collected in support of this sampling program. This section includes detailed information on the analysis of duff and and tree bark, as well as the data reporting requirements, sample holding times, and custody procedures. An analytical requirements summary sheet (NEFOREST-0812), which details the specific preparation and analytical requirements associated with this sampling program, is provided in Appendix D. The analytical requirements summary sheet will be reviewed and approved by all participating laboratories in this sampling program prior to any sample handling. A copy of this analytical requirements summary sheet will be submitted with each COC. The personal air samples collected for the on-going health and safety monitoring will be analyzed in accordance with the Response Action SAP (CDM Xxxxx 2011). In brief, air samples will be prepared and analyzed by PCM in accordance with NIOSH Method 7400, Issue 2.
