Post-mortem study Sample Clauses

Post-mortem study. Post-mortem studies will be performed to characterize the internal components after formation and after cycling. Such study implicates a set of methods of electrochemical, physicochemical and structural characterization of materials and components (positive and negative electrodes, separator, electrolyte) at different scales to identify precisely the mechanisms which are involved and which cause degradation 9 . Figure 5 illustrates the different techniques of characterization that are performed for each of the bulk or surface components. Note that separator is specified to generalize to all systems but is not to be considered for solid state. It is the complementarity of the information obtained with these techniques that helps to understand the origin of the degradation and the resulting performance losses. Figure 5 - Physicochemical characterization techniques and phenomena they are able to detect. Green, orange, and red colors indicate good, limited, and no capability for detection of a specific aging mechanism, respectively9. The preparation of the samples requires the dismantling of cell in a glove box in an inert atmosphere (with argon to obtain low levels of H2O and O2). Thus, the internal components are not in contact with the air, thus preserving their condition as it was in the cell after operation. The cell is always dismantled at a fully discharged state, on the one hand for safety reasons, and on the other hand to characterize the cells at an identical state of charge between fresh and aged electrodes.
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Related to Post-mortem study

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