Synthesis of well Sample Clauses

Synthesis of well defined nanomaterials To develop reliable results in safety testing and innovation requires the synthesis, characterization, and modification of well-defined nanomaterials. This could include the development and provision of a set of standard materials for interlaboratory comparisons and benchmark reference points for theoretical and experimental studies. Development of reproducible, scalable methods for synthesizing nanomaterials with precisely controlled chemical and physical properties and the availability of sample sets that vary by only single properties (e.g., size, surface groups, shape) could significantly advance our understanding of how these properties affect response outcomes. The availability of such well-defined MNMs would represent a potential market for both researchers and innovators working towards Safe-by-Design. The production and provision of both MNMs for use as both safety testing reference materials and materials for innovation chains therefore represents a potential business opportunity.
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Synthesis of well defined principal microcapsule polymers) The principal microcapsule polymers sodium cellulose sulfate (SCS) and poly(methylene-co-cyanoguanidine) (PMCG) will be synthesized in the subcontractor’s laboratory at the Institute of Macromolecular Chemistry in Prague. SCS will be formed by sulfation of the cellulose hydroxyl groups with a mild sulfation agent, SO3.DMF, which ensures low degradation of cellulose backbone and high degrees of substitution. Different sources of cellulose will be used thus achieving a library of SCS with vastly different molecular weights. The backbone of the low-molecular weight polycation, PMCG, is formed by condensation of cyanoguanidine and paraformaldehyde in the presence of NH4Cl. The role of NH4Cl is two-fold; it ensures the pH at which oligomeric, linear products are formed, and, at the same time, reacts with the cyano group of cyanoguanidine, which increases the charge density at the resulting condensate.
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